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        EESemi.com Forum Archives 
		
		Decapsulation 
		Dilemma - Melting Copper Wires 
                       
        
        
        
        
        
                
        
        
              
		        
         
        
        
        
        
        
        
        
        
        
        
        
        Proper device
		failure analysis can not be performed unless 
		the sample can be decapsulated nicely.  Different plastic molding 
		compounds and the internal features of the device react to the 
		decapsulating etchant in different ways. As such, successful
		decapsulation of the part requires that the 
		correct etchant recipe is applied.  
		But what if a failure analysis lab's standard recipes can not 
		decapsulate a new device? The archived forum thread below discusses the 
		decapsulation dilemma of the thread starter, who observed that the 
		copper wires of his sample is being dissolved by the etchant he was 
		using. 
		
            
        
		
			
				
				
					
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						Posted by Rivs: Wed 
						Aug 08, 2007 10:49 am    Post 
						subject: HYSOL MG15F MOLDING COMPOUND  | 
					 
					
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						Guys need your idea on 
						this.... We currently have an evaluation on copper wire 
						bonding (2 mils) the problem is during failure analysis 
						chemical decapsulation, copper wire were 
						etched/dissolved after the unit is fully decapped using 
						sulfuric acid. As experienced MG15F molding compound 
						does not react on Nitric red fuming.  
						 
						Hope you can give us any idea on how we can decap the 
						parts without over etching/dissolving the copper wire.
						 
						 
						Thanks.   | 
					 
				 
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						Posted by Paulpang: 
						Thu Aug 09, 2007 8:37 pm   
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						Hi Rivs:  
						 
						Try to use the formula: Sulfuric acid : nitric acid= 3 
						:1 or (2:1)  
						I am also working on copper wire decap in recently. Good 
						luck in your FA process.  
						 
						regards,  
						paul  | 
					 
				 
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						Posted by Paulpang: 
						Thu Aug 09, 2007 8:39 pm   
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						Take note: sulfruic acid (96%), 
						nitric acid (98%)-----paul  | 
					 
				 
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						Posted by Rivs: Fri 
						Aug 10, 2007 8:23 am    Post 
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						Hi Paul, Thanks for the 
						response. I'll try this and give you feedback on the 
						result. Anyway fyi I'ved tried this mixture in a 9:1 and 
						5:1 ration (Nitric:Sulfuric) but none of them worked.
						 
						 
						Again thanks.   | 
					 
				 
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						Posted by Paulpang: 
						Sat Aug 11, 2007 7:41 pm   
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						Hi Rivs:  
						The decap you finished by manual decap or auto decap? I 
						carried out it by manual. Keep in touch....  
						 
						regards,  
						paul  | 
					 
				 
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						Posted by Rivs: Mon 
						Aug 13, 2007 3:55 pm    Post 
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						Hi paul, I am doing it 
						manually by submerssion method, the ratio you gave 
						did'nt work, the Nitric acid just vaporized and the 
						package of the unit is still solid, just like our 
						mixture of 5:1 (Nitric:Sulfuric), are you successfull 
						with what you did?   | 
					 
				 
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						Posted by Paulpang: 
						Mon Aug 13, 2007 8:44 pm   
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						Hi Rivs:  
						It will be easy to control if you perform decap by 
						manual. If the compound can not dissolve then,  
						1.) take the unit out of chemical.  
						2.) use aceton to wash the unit  
						3.) put the unit into chemical again  
						4.) compound still can not dissolve  
						repeat step 1 to 4.  
						thus, you'll find differnce.  
						 
						By the way, what temperature did you set ? 250 deg would 
						be prefered.  
						 
						regards,  
						paul  | 
					 
					
        
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